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The Microanalysis System

What makes a Good Detector?

The Pulse Processor

 

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Role of the pulse processor
Analog pulse shaping
Time variant shaping
Digital pulse shaping
Fixed process time
Adaptive pulse shaping
Resolution & count rate
Pulse pile-up protection
Comparing different pulse processors
Summary

 

The pulse processor

 

Summary

 

  •  Both detector and pulse processor are equally important parts of the measurement chain

  •  Pulse processor performance is characterized by the maximum acquisition rate and resolution achievable at each process time

  •  Measuring the change in energy calibration and resolution as the count rate changes shows how reliably the measurement chain will provide accurate data for automatic peak identification and standardless quantitative analysis

  •  Even small changes in resolution or energy calibration can lead to large errors when analyzing severely overlapped X-ray lines

 

References

 

 K. Kandiah, A. J. Smith and G. White, IEEE Trans. Nucl. Sci., NS-22, 2058 (1975)

 P.J. Statham, In Proceedings NIST-MAS Special Topics Workshop, “Understanding the Accuracy Barrier in Quantitative Electron Probe Microanalysis and the Role of Standards” NIST, Gaithersburg, MD, USA, April 8-11, (2002)

 

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